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0 votes
0 answers
107 views

Selective Removal of Sodium Acetate

I am currently working on an extraction and synthesis of sodium salicyate from acetylsalicylic acid and sodium hydroxide. After doing a liquid-liquid extraction from DCM, using a sodium hydroxide ...
Sam Albury's user avatar
3 votes
2 answers
1k views

How do you achieve phase separation of a methanol / chloroform solution?

If I'm washing a methanol solution with chloroform, can I just add water in a 1:1 mixture with the methanol and expect it to break? Do I need to do anything else to cause the aqueous phase to separate ...
Sargun Dhillon's user avatar
8 votes
2 answers
1k views

Looking for caffeine partition coefficients

As part of a project, I'm looking to carry out a liquid-liquid extraction of caffeine from an aqueous phase to an organic phase, using dichloromethane or ethyl acetate. So I'm looking for the ...
Eli's user avatar
  • 155
1 vote
3 answers
69 views

When an aqueous extract of a substance is said to be administered at a certain quantity, is the quoted mass analogous to one as original substance?

I'm trying to read studies about the possible toxicity of the leaves of some plant often said to possess positive medicinal properties. In the studies, performed on rats, it is usually said that an ...
TLSO's user avatar
  • 147
5 votes
1 answer
807 views

How can I measure the amount of quinine in a home-made tonic water?

I'm into mixology, and lately I've been looking into experimenting with home-made tonic water, by extracting quinine (quinine salts) from cinchona barks in an acidic aqueous solution. I've read a bit ...
zetaprime's user avatar
  • 145
5 votes
0 answers
159 views

Where is my antimony going?

I work in a trace metals laboratory operating an ICP-OES. I've been having some trouble with the recovery of antimony in a weak $\ce{HCl}$ solution post-digestion. The antimony is part of a mix of ...
Max Power's user avatar
2 votes
1 answer
874 views

Trying to displace iron from ferrous sulphate heptahydrate using aluminium foil but nothing has happened

I started by dissolving the sulphate into water and filtering it as I noticed there was a dirty residue lying at the bottom. (I am using ferrous sulphate that is commonly used in gardening.) I then ...
The Garage Chemist's user avatar
3 votes
1 answer
553 views

Can we extract KI from Lugol solution?

I want to extract the $\ce{KI}$ component of the Lugol solution, is there a method to do it? If not, how can I make a $\ce{KI}$ solution?
Pedro's user avatar
  • 161