All Questions
Tagged with extraction organic-chemistry
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How does a conc. electrolyte solution extract water from a organic phase like diethyl ether or ethyl acetate?
In organic chemistry, often, during the last steps of a workup we use concentrated brine solution (NaCl) to "extract" the water from the organic layer, especially when we have an organic ...
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TsOH and 5% NaHCO3 Interaction: Unexpected Dark Green Color
Here's the brief:
I synthesized alkyl gallates (ethyl gallate, butyl gallate, and amyl gallate) using Fischer esterification.
I used TsOH instead of concentrated H2SO4 as the catalyst.
After ...
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2
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Liquid-liquid extraction of sorbicillinol in water with ethyl acetate
My solution consisted of sorbicillinol and water, sorbicillinol being a polar substance. I wanted to isolate sorbicillinol from water using liquid-liquid extraction.
For my solvent I used ethyl ...
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1
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Decarboxylation of THCA in cannabis after plant material is mixed with ethanol [closed]
When making a tincture of cannabis, an early step is decarboxylation by roasting cannabis flowers at low temperatures (such as 230F for 30 minutes). My question is, how can one decarboxylate cannabis ...
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BTX nitration work-up
I'm trying to understand washing step in a btx nitration process. In all these processes the work-up streams are very similar. The reaction mixture passes from the nitrator to a separator or ...
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1
answer
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Natural Sources for S-(-)-Limonene?
I'm interested in developing an undergrad organic lab that delves deeper into distillation/extraction, optical rotation and enantiomers. Our lab currently does a steam distillation extracting R-(+)-...
3
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2
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How do you achieve phase separation of a methanol / chloroform solution?
If I'm washing a methanol solution with chloroform, can I just add water in a 1:1 mixture with the methanol and expect it to break? Do I need to do anything else to cause the aqueous phase to separate ...
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Looking for caffeine partition coefficients
As part of a project, I'm looking to carry out a liquid-liquid extraction of caffeine from an aqueous phase to an organic phase, using dichloromethane or ethyl acetate.
So I'm looking for the ...
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Are there any tests which distinguish between triglycerides and polar lipids/impurities that can be conducted in a high school setting?
I am currently writing a research essay about using a mixed polar (methanol) and non-polar (heptane) solvent system to extract oil from mango seed kernels. One of the difficulties of using polar ...
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Related to liquid-liquid extraction
I was reading about purification of organic compounds and I came across this.
I quote below, a line from the excerpt that caused my confusion.
The organic solvent is later removed by distillation or ...
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How do i get acetic acid from vinegar?
I'm trying to improve my rocket project, but, since the competition only allows the use of vinegar and sodium bicarbonate as its fuel, I had an idea of using the vinegar in a different way. My plan ...
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Choise of solvent for extraction
In the synthesis of (S)-Diphenyl(pyrrolidine-2yl)methanol, I need to extract the product using an organic solvent and water. Which organic solvent is the most suitable in this case?
Ethyl acetate: I ...
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406
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Looking for advice regarding a larger scale soxhlet extraction
I have successfully completed a few soxhlet extractions at a much smaller scale using a soxhlet extractor with ~200ml capacity. With that, I was able to extract from ~100g of pre-powdered, sonicated ...
6
votes
1
answer
292
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Decarboxylation of THCA during CO2 Extraction of Cannabis
We have a strange problem. We are performing CO2 extraction on cannabis and we are seeing considerable decarboxylation of THCA to THC.
We have high quality temperature sensors at the heat exchangers, ...
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How many times should I run a solvent extration experiment through?
For advanced higher chemistry project, I am extracting cinnamaldehyde from cinnamon via first steam distillation and then solvent extraction using hexane. I'll be adding sodium chloride to the water/...
