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How can I set up and process my excitation-emission matrices properly?

I'm running EEMS on some water samples on a Horiba Fluoromax 4 spectrofluorometer. Method below. $\pu{240-580nm}$ emission, $\pu{5nm}$ interval, $\pu{1nm}$ width. $\pu{240-480nm}$ excitation, $\pu{...
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