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Tagged with electroplating oxidation-state
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Is there any method to make sure a electroplated layer of iron oxidizes into magnetite (Fe3O4) instead of hematite (Fe2O3)?
I am currently electroplating iron on copper using a DIY setup in my lab. Steel sheet as anode with electrolyte having 5% acetic acid with sodium carbonate to form sodium acetate and added some NaCl ...