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Sep 16, 2022 at 22:14 comment added user55119 You started with a nitrogen atmosphere. Did you purge with hydrogen? Parr apparatus should be in a hood.
Sep 16, 2022 at 20:33 review Close votes
Oct 13, 2022 at 16:08
Sep 16, 2022 at 20:18 comment added jimchmst I agree, the few hydrogenations I have done were at low pressure and ambient T. The reaction was smooth and fast, monitored by the lowering of H2 pressure. Research some methods in the library not the internet
Sep 16, 2022 at 18:41 history edited Mathew Mahindaratne CC BY-SA 4.0
Improved the heading and clarity. Added some tags.
Sep 16, 2022 at 18:31 answer added Mathew Mahindaratne timeline score: 1
Sep 16, 2022 at 6:21 comment added Waylander This is a simple reaction that should work easily at much lower pressures. Have you tried using a different batch of catalyst? Have other researchers used this batch successfully recently?
S Sep 16, 2022 at 3:08 review First questions
Sep 16, 2022 at 14:38
S Sep 16, 2022 at 3:08 history asked Greg CC BY-SA 4.0